Structures by: Boudon C.

Total: 57

C41H34Cl2N2O2Si,C4H8O2

C41H34Cl2N2O2Si,C4H8O2

London, Gáborvon Wantoch Rekowski, MargareteDumele, OliverSchweizer, W. BerndGisselbrecht, Jean-PaulBoudon, CorinneDiederich, François

Chemical Science (2014) 5, 3 965

a=20.094(7)Å   b=17.545(6)Å   c=24.430(8)Å

α=90°   β=112.452(5)°   γ=90°

C39H36N4Si

C39H36N4Si

London, Gáborvon Wantoch Rekowski, MargareteDumele, OliverSchweizer, W. BerndGisselbrecht, Jean-PaulBoudon, CorinneDiederich, François

Chemical Science (2014) 5, 3 965

a=8.265(2)Å   b=11.375(3)Å   c=17.895(4)Å

α=105.856(9)°   β=99.890(9)°   γ=94.670(10)°

C33H36Si

C33H36Si

London, Gáborvon Wantoch Rekowski, MargareteDumele, OliverSchweizer, W. BerndGisselbrecht, Jean-PaulBoudon, CorinneDiederich, François

Chemical Science (2014) 5, 3 965

a=8.8447(4)Å   b=18.3363(9)Å   c=17.4324(6)Å

α=90°   β=114.902(2)°   γ=90°

C39H38O2Si1

C39H38O2Si1

London, Gáborvon Wantoch Rekowski, MargareteDumele, OliverSchweizer, W. BerndGisselbrecht, Jean-PaulBoudon, CorinneDiederich, François

Chemical Science (2014) 5, 3 965

a=14.703(15)Å   b=14.833(16)Å   c=15.051(16)Å

α=85.804(18)°   β=87.160(19)°   γ=66.309(15)°

C33H34O2Si,0.25(C4H10O)

C33H34O2Si,0.25(C4H10O)

London, Gáborvon Wantoch Rekowski, MargareteDumele, OliverSchweizer, W. BerndGisselbrecht, Jean-PaulBoudon, CorinneDiederich, François

Chemical Science (2014) 5, 3 965

a=38.218(8)Å   b=19.296(4)Å   c=8.5140(18)Å

α=90°   β=90.665(4)°   γ=90°

C26H24N6,CH4O

C26H24N6,CH4O

Chiu, MelanieJaun, BernhardBeels, Marten T. R.Biaggio, IvanGisselbrecht, Jean-PaulBoudon, CorinneSchweizer, W. BerndKivala, MilanDiederich, François

Organic letters (2012) 14, 1 54-57

a=12.3190(3)Å   b=14.5330(3)Å   c=16.0170(4)Å

α=64.0820(11)°   β=69.3300(11)°   γ=66.1260(13)°

C30H26N6

C30H26N6

Chiu, MelanieJaun, BernhardBeels, Marten T. R.Biaggio, IvanGisselbrecht, Jean-PaulBoudon, CorinneSchweizer, W. BerndKivala, MilanDiederich, François

Organic letters (2012) 14, 1 54-57

a=26.6002(6)Å   b=12.4004(8)Å   c=17.7239(12)Å

α=90.00°   β=120.646(5)°   γ=90.00°

2(C24H19N5),C7H8

2(C24H19N5),C7H8

Chiu, MelanieJaun, BernhardBeels, Marten T. R.Biaggio, IvanGisselbrecht, Jean-PaulBoudon, CorinneSchweizer, W. BerndKivala, MilanDiederich, François

Organic letters (2012) 14, 1 54-57

a=7.2402(13)Å   b=11.587(2)Å   c=13.950(4)Å

α=89.683(8)°   β=78.116(9)°   γ=74.635(13)°

2(C728H28N6),C18H20N2,C1H4O

2(C728H28N6),C18H20N2,C1H4O

Chiu, MelanieJaun, BernhardBeels, Marten T. R.Biaggio, IvanGisselbrecht, Jean-PaulBoudon, CorinneSchweizer, W. BerndKivala, MilanDiederich, François

Organic letters (2012) 14, 1 54-57

a=11.5040(7)Å   b=12.1136(7)Å   c=12.8530(8)Å

α=100.552(2)°   β=98.525(2)°   γ=96.793(3)°

C36H26

C36H26

Rivera-Fuentes, PabloRekowski, Margarete von WantochSchweizer, W. BerndGisselbrecht, Jean-PaulBoudon, CorinneDiederich, François

Organic letters (2012) 14, 16 4066-4069

a=10.6839(3)Å   b=23.5559(7)Å   c=10.7016(3)Å

α=90.00°   β=115.2010(10)°   γ=90.00°

C30H20,CH4O

C30H20,CH4O

Rivera-Fuentes, PabloRekowski, Margarete von WantochSchweizer, W. BerndGisselbrecht, Jean-PaulBoudon, CorinneDiederich, François

Organic letters (2012) 14, 16 4066-4069

a=25.324(11)Å   b=25.324Å   c=5.877(3)Å

α=90.00°   β=90.00°   γ=120.00°

C84H62N8O2Zn,2(CHCl3),H2O

C84H62N8O2Zn,2(CHCl3),H2O

Lo, MamadouMahajan, DineshWytko, Jennifer A.Boudon, CorinneWeiss, Jean

Organic letters (2009) 11, 12 2487-2490

a=12.7416(3)Å   b=13.0016(3)Å   c=23.9379(7)Å

α=77.8380(10)°   β=86.0080(10)°   γ=69.139(2)°

C15H10N4

C15H10N4

Nicolle N. P. MoonenRobin GistCorinne BoudonJean-Paul GisselbrechtPaul SeilerTsuyoshi KawaiAtsushi KishiokaMaurice GrossMasahiro IrieFrançois Diederich

Org. Biomol. Chem. (2003) 1, 12 2032-2034

a=7.014(1)Å   b=7.085(1)Å   c=14.149(2)Å

α=77.79(2)°   β=89.21(1)°   γ=77.40(2)°

C24H20N4

C24H20N4

Nicolle N. P. MoonenRobin GistCorinne BoudonJean-Paul GisselbrechtPaul SeilerTsuyoshi KawaiAtsushi KishiokaMaurice GrossMasahiro IrieFrançois Diederich

Org. Biomol. Chem. (2003) 1, 12 2032-2034

a=3.9477(2)Å   b=11.1064(4)Å   c=22.3725(9)Å

α=90.00°   β=93.769(2)°   γ=90.00°

(E)-2-(3-(4-bromophenyl)-1-(4- (dimethylamino)phenyl)allylidene)malononitrile

C20H16BrN3

Jarowski, Peter D.Wu, Yi-LinBoudon, CorinneGisselbrecht, Jean-PaulGross, MauriceSchweizer, W. BerndDiederich, François

Organic & Biomolecular Chemistry (2009) 7, 7 1312-1322

a=9.4778(3)Å   b=7.9420(3)Å   c=24.0757(9)Å

α=90.00°   β=93.4125(14)°   γ=90.00°

2-(1-(4-(dimethylamino)phenyl)-3-(4- methoxyphenyl)allylidene)propanedinitrile

C21H19N3O

Jarowski, Peter D.Wu, Yi-LinBoudon, CorinneGisselbrecht, Jean-PaulGross, MauriceSchweizer, W. BerndDiederich, François

Organic & Biomolecular Chemistry (2009) 7, 7 1312-1322

a=7.8176(2)Å   b=15.0473(4)Å   c=16.0532(5)Å

α=104.702(2)°   β=90.581(2)°   γ=104.638(2)°

C70H40N2

C70H40N2

Mitzel, FriederBoudon, CorinneGisselbrecht, Jean-PaulSeiler, PaulGross, MauriceDiederich, François

Chemical Communications (Cambridge, United Kingdom) (2003) 14 1634-1635

a=13.6643(5)Å   b=14.0449(6)Å   c=15.9105(8)Å

α=66.12(1)°   β=68.03(1)°   γ=83.06(1)°

(E)-2-(3-cyclohexyl-1-(4- (dimethylamino)phenyl)allylidene)malononitrile

C20H23N3

Jarowski, Peter D.Wu, Yi-LinBoudon, CorinneGisselbrecht, Jean-PaulGross, MauriceSchweizer, W. BerndDiederich, François

Organic & Biomolecular Chemistry (2009) 7, 7 1312-1322

a=10.0678(3)Å   b=15.9325(5)Å   c=11.7652(4)Å

α=90.00°   β=111.406(2)°   γ=90.00°

C70H40N2

C70H40N2

Mitzel, FriederBoudon, CorinneGisselbrecht, Jean-PaulSeiler, PaulGross, MauriceDiederich, François

Chemical Communications (Cambridge, United Kingdom) (2003) 14 1634-1635

a=13.6643(5)Å   b=14.0449(6)Å   c=15.9105(8)Å

α=66.12(1)°   β=68.03(1)°   γ=83.06(1)°

C22H15N5

C22H15N5

Kivala, MilanBoudon, CorinneGisselbrecht, Jean-PaulSeiler, PaulGross, MauriceDiederich, François

Chemical communications (Cambridge, England) (2007) 45 4731-4733

a=8.8680(13)Å   b=9.2552(14)Å   c=11.7022(14)Å

α=101.406(2)°   β=93.315(12)°   γ=94.983(2)°

3(C28H19N5),1.5(C2H2Cl4)

3(C28H19N5),1.5(C2H2Cl4)

Kivala, MilanBoudon, CorinneGisselbrecht, Jean-PaulSeiler, PaulGross, MauriceDiederich, François

Chemical communications (Cambridge, England) (2007) 45 4731-4733

a=11.1429(14)Å   b=16.3191(15)Å   c=22.2110(17)Å

α=82.970(11)°   β=85.747(12)°   γ=81.416(11)°

C27H21N7

C27H21N7

Govindasamy JayamuruganJean-Paul GisselbrechtCorinne BoudonFranziska SchoenebeckW. Bernd SchweizerBruno BernetFrancois Diederich

Chem.Commun. (2011) 47, 4520

a=11.2924(4)Å   b=15.4265(7)Å   c=25.3239(11)Å

α=90.00°   β=90.00°   γ=90.00°

C27H21N7

C27H21N7

Govindasamy JayamuruganJean-Paul GisselbrechtCorinne BoudonFranziska SchoenebeckW. Bernd SchweizerBruno BernetFrancois Diederich

Chem.Commun. (2011) 47, 4520

a=23.1039(7)Å   b=6.0491(2)Å   c=15.7821(5)Å

α=90.00°   β=92.218(2)°   γ=90.00°

C17H10N6

C17H10N6

Govindasamy JayamuruganJean-Paul GisselbrechtCorinne BoudonFranziska SchoenebeckW. Bernd SchweizerBruno BernetFrancois Diederich

Chem.Commun. (2011) 47, 4520

a=11.5737(3)Å   b=11.5737(3)Å   c=11.5001(5)Å

α=90.00(0)°   β=90.0(0)°   γ=90.00(0)°

2(C26H20N6),CHCl3

2(C26H20N6),CHCl3

Govindasamy JayamuruganJean-Paul GisselbrechtCorinne BoudonFranziska SchoenebeckW. Bernd SchweizerBruno BernetFrancois Diederich

Chem.Commun. (2011) 47, 4520

a=9.1282(3)Å   b=11.1896(3)Å   c=12.4251(4)Å

α=102.4170(13)°   β=90.4984(13)°   γ=103.9678(13)°

2(C25H21N5),0.5(C2H4Cl2)

2(C25H21N5),0.5(C2H4Cl2)

Govindasamy JayamuruganJean-Paul GisselbrechtCorinne BoudonFranziska SchoenebeckW. Bernd SchweizerBruno BernetFrancois Diederich

Chem.Commun. (2011) 47, 4520

a=9.8044(6)Å   b=12.8651(10)Å   c=18.011(2)Å

α=93.245(5)°   β=91.748(5)°   γ=109.113(3)°

C16H11N5

C16H11N5

Francois DiederichIvan BiaggioCorinne BoudonJean-Paul GisselbrechtMaurice GrossJ.H. LimJoshua C. MayTsuyoshi MichinobuPaul Seiler

Chemical Communications (2005)

a=10.7459(2)Å   b=11.0754(3)Å   c=15.1601(5)Å

α=70.935(1)°   β=71.461(1)°   γ=61.437(2)°

C26H20N6,2(CH2Cl2)

C26H20N6,2(CH2Cl2)

Francois DiederichIvan BiaggioCorinne BoudonJean-Paul GisselbrechtMaurice GrossJ.H. LimJoshua C. MayTsuyoshi MichinobuPaul Seiler

Chemical Communications (2005)

a=7.3661(1)Å   b=9.5653(2)Å   c=20.8690(4)Å

α=91.580(8)°   β=95.014(7)°   γ=92.986(9)°

C24H20N6

C24H20N6

Francois DiederichIvan BiaggioCorinne BoudonJean-Paul GisselbrechtMaurice GrossJ.H. LimJoshua C. MayTsuyoshi MichinobuPaul Seiler

Chemical Communications (2005)

a=15.0448(7)Å   b=15.9323(8)Å   c=17.1300(8)Å

α=90.00°   β=90.00°   γ=90.00°

C14H11N3

C14H11N3

Francois DiederichIvan BiaggioCorinne BoudonJean-Paul GisselbrechtMaurice GrossJ.H. LimJoshua C. MayTsuyoshi MichinobuPaul Seiler

Chemical Communications (2005)

a=4.0006(3)Å   b=17.9661(10)Å   c=17.145(2)Å

α=90.00°   β=96.308(3)°   γ=90.00°

C40H36N10,0.25(CH2Cl2)

C40H36N10,0.25(CH2Cl2)

Breiten, BenjaminWu, Yi-LinJarowski, Peter D.Gisselbrecht, Jean-PaulBoudon, CorinneGriesser, MarkusOnitsch, ChristineGescheidt, GeorgSchweizer, W. BerndLanger, NicolleLennartz, ChristianDiederich, François

Chemical Science (2011) 2, 1 88

a=13.6680(6)Å   b=12.3175(6)Å   c=24.2737(12)Å

α=90.00°   β=100.887(2)°   γ=90.00°

C28H24I3N3

C28H24I3N3

Dengiz, CagatayBreiten, BenjaminGisselbrecht, Jean-PaulBoudon, CorinneTrapp, NilsSchweizer, W. BerndDiederich, François

The Journal of organic chemistry (2015) 80, 2 882-896

a=28.5414(12)Å   b=6.3924(3)Å   c=31.3881(14)Å

α=90.00°   β=109.225(2)°   γ=90.00°

C28H24Br3N3

C28H24Br3N3

Dengiz, CagatayBreiten, BenjaminGisselbrecht, Jean-PaulBoudon, CorinneTrapp, NilsSchweizer, W. BerndDiederich, François

The Journal of organic chemistry (2015) 80, 2 882-896

a=7.1349(4)Å   b=11.2698(5)Å   c=16.4853(8)Å

α=79.288(2)°   β=87.269(3)°   γ=79.285(2)°

C35H30Fe2Si,CHCl3

C35H30Fe2Si,CHCl3

Dengiz, CagatayBreiten, BenjaminGisselbrecht, Jean-PaulBoudon, CorinneTrapp, NilsSchweizer, W. BerndDiederich, François

The Journal of organic chemistry (2015) 80, 2 882-896

a=7.8579(12)Å   b=10.9549(15)Å   c=19.720(3)Å

α=75.763(5)°   β=80.428(5)°   γ=80.484(5)°

C29H23N7,HCl3

C29H23N7,HCl3

Jayamurugan, GovindasamyFinke, Aaron D.Gisselbrecht, Jean-PaulBoudon, CorinneSchweizer, W. BerndDiederich, François

The Journal of organic chemistry (2014) 79, 1 426-431

a=9.1862(3)Å   b=11.9442(5)Å   c=14.8114(5)Å

α=106.527(2)°   β=97.798(2)°   γ=110.162(2)°

C25H19N5O

C25H19N5O

Jayamurugan, GovindasamyFinke, Aaron D.Gisselbrecht, Jean-PaulBoudon, CorinneSchweizer, W. BerndDiederich, François

The Journal of organic chemistry (2014) 79, 1 426-431

a=11.2869(8)Å   b=11.7092(8)Å   c=7.9701(5)Å

α=90.00°   β=95.891(3)°   γ=90.00°

C29H23N7

C29H23N7

Jayamurugan, GovindasamyFinke, Aaron D.Gisselbrecht, Jean-PaulBoudon, CorinneSchweizer, W. BerndDiederich, François

The Journal of organic chemistry (2014) 79, 1 426-431

a=8.9930(8)Å   b=9.8212(9)Å   c=15.1041(14)Å

α=94.013(5)°   β=96.665(4)°   γ=109.521(4)°

C38H34Cl2N8

C38H34Cl2N8

Jayamurugan, GovindasamyFinke, Aaron D.Gisselbrecht, Jean-PaulBoudon, CorinneSchweizer, W. BerndDiederich, François

The Journal of organic chemistry (2014) 79, 1 426-431

a=10.9767(4)Å   b=11.4460(6)Å   c=16.6130(8)Å

α=94.177(2)°   β=93.6006(13)°   γ=106.993(2)°

C38H46N6

C38H46N6

Jayamurugan, GovindasamyFinke, Aaron D.Gisselbrecht, Jean-PaulBoudon, CorinneSchweizer, W. BerndDiederich, François

The Journal of organic chemistry (2014) 79, 1 426-431

a=9.8523(3)Å   b=28.5180(11)Å   c=13.2470(5)Å

α=90.00°   β=111.422(2)°   γ=90.00°

C26H22N6

C26H22N6

Jayamurugan, GovindasamyFinke, Aaron D.Gisselbrecht, Jean-PaulBoudon, CorinneSchweizer, W. BerndDiederich, François

The Journal of organic chemistry (2014) 79, 1 426-431

a=12.9058(13)Å   b=7.5529(7)Å   c=12.7458(10)Å

α=90.00°   β=118.198(3)°   γ=90.00°

C34H19FeN9

C34H19FeN9

Benjamin BreitenMarkus JordanDaisuke TauraMichal ZaliberaMarkus GriesserDaria ConfortinCorinne BoudonJean-Paul GisselbrechtW. Bernd SchweizerGeorg GescheidtFrançois Diederich

Journal of Organic Chemistry (2013) 78, 1760-1767

a=7.4036(5)Å   b=40.272(3)Å   c=9.8627(6)Å

α=90.00°   β=104.307(5)°   γ=90.00°

C52H28N10,2(CH2Cl2)

C52H28N10,2(CH2Cl2)

Benjamin BreitenMarkus JordanDaisuke TauraMichal ZaliberaMarkus GriesserDaria ConfortinCorinne BoudonJean-Paul GisselbrechtW. Bernd SchweizerGeorg GescheidtFrançois Diederich

Journal of Organic Chemistry (2013) 78, 1760-1767

a=8.480(3)Å   b=15.471(4)Å   c=18.112(5)Å

α=91.016(7)°   β=94.203(8)°   γ=93.318(8)°

C41H24F3N3,CHCl3

C41H24F3N3,CHCl3

Yi-Lin WuMihaiela C. StuparuCorinne BoudonJean-Paul GisselbrechtW. Bernd SchweizerKim K. BaldridgeJay S. SiegelFrançois Diederich

Journal of Organic Chemistry (2012) 77, 11014-11026

a=11.8172(15)Å   b=14.954(2)Å   c=20.549(3)Å

α=70.961(5)°   β=84.168(5)°   γ=88.955(5)°

C42H31N3

C42H31N3

Aaron D. FinkeOliver DumeleMichal ZaliberaDaria ConfortinPawel CiasGovindasamy JayamuruganJean-Paul GisselbrechtCorinne BoudonW. Bernd SchweizerGeorg GescheidtFrançois Diederich

Journal of the American Chemical Society (2012) 134, 18139-18146

a=10.1004(3)Å   b=10.1085(3)Å   c=15.9835(4)Å

α=77.1840(10)°   β=89.472(2)°   γ=76.6920(10)°

C52H84N2Si4

C52H84N2Si4

Aaron D. FinkeOliver DumeleMichal ZaliberaDaria ConfortinPawel CiasGovindasamy JayamuruganJean-Paul GisselbrechtCorinne BoudonW. Bernd SchweizerGeorg GescheidtFrançois Diederich

Journal of the American Chemical Society (2012) 134, 18139-18146

a=13.2013(7)Å   b=14.5468(7)Å   c=14.6172(7)Å

α=90.00°   β=106.826(2)°   γ=90.00°

C70H104N4Si4

C70H104N4Si4

Aaron D. FinkeOliver DumeleMichal ZaliberaDaria ConfortinPawel CiasGovindasamy JayamuruganJean-Paul GisselbrechtCorinne BoudonW. Bernd SchweizerGeorg GescheidtFrançois Diederich

Journal of the American Chemical Society (2012) 134, 18139-18146

a=47.9783(16)Å   b=47.9783(16)Å   c=16.4921(7)Å

α=90.00°   β=90.00°   γ=120.00°

C26H20N6,CH2Cl2

C26H20N6,CH2Cl2

Govindasamy JayamuruganOliver DumeleJean-Paul GisselbrechtCorinne BoudonW. Bernd SchweizerBruno BernetFrançois Diederich

Journal of the American Chemical Society (2013) 135, 3599-3606

a=13.1343(5)Å   b=8.4280(4)Å   c=22.6288(10)Å

α=90.00°   β=95.780(2)°   γ=90.00°

C36H31N7

C36H31N7

Govindasamy JayamuruganOliver DumeleJean-Paul GisselbrechtCorinne BoudonW. Bernd SchweizerBruno BernetFrançois Diederich

Journal of the American Chemical Society (2013) 135, 3599-3606

a=10.8943(4)Å   b=14.1475(6)Å   c=19.8825(8)Å

α=90.00°   β=103.698(2)°   γ=90.00°

C46H42N8,CH2Cl2

C46H42N8,CH2Cl2

Govindasamy JayamuruganOliver DumeleJean-Paul GisselbrechtCorinne BoudonW. Bernd SchweizerBruno BernetFrançois Diederich

Journal of the American Chemical Society (2013) 135, 3599-3606

a=10.6434(6)Å   b=13.6284(8)Å   c=14.4880(9)Å

α=79.959(3)°   β=84.754(3)°   γ=88.332(3)°

3(C36H31N7,CHCl3

3(C36H31N7,CHCl3

Govindasamy JayamuruganOliver DumeleJean-Paul GisselbrechtCorinne BoudonW. Bernd SchweizerBruno BernetFrançois Diederich

Journal of the American Chemical Society (2013) 135, 3599-3606

a=16.0228(11)Å   b=16.8314(11)Å   c=17.8423(11)Å

α=80.594(2)°   β=81.100(3)°   γ=80.250(2)°

C44H40N8,4(C7H8)

C44H40N8,4(C7H8)

Govindasamy JayamuruganOliver DumeleJean-Paul GisselbrechtCorinne BoudonW. Bernd SchweizerBruno BernetFrançois Diederich

Journal of the American Chemical Society (2013) 135, 3599-3606

a=15.2956(9)Å   b=19.8622(10)Å   c=19.6049(9)Å

α=90.00°   β=93.109(2)°   γ=90.00°

C70H66

C70H66

Cao, JingLondon, GáborDumele, Olivervon Wantoch Rekowski, MargareteTrapp, NilsRuhlmann, LaurentBoudon, CorinneStanger, AmnonDiederich, François

Journal of the American Chemical Society (2015) 137, 22 7178-7188

a=12.8654(8)Å   b=18.9405(10)Å   c=24.2937(14)Å

α=111.777(4)°   β=90.520(5)°   γ=90.037(5)°

C74H76O4,6(CDCl3)

C74H76O4,6(CDCl3)

Cao, JingLondon, GáborDumele, Olivervon Wantoch Rekowski, MargareteTrapp, NilsRuhlmann, LaurentBoudon, CorinneStanger, AmnonDiederich, François

Journal of the American Chemical Society (2015) 137, 22 7178-7188

a=16.3401(9)Å   b=10.9180(7)Å   c=27.3803(15)Å

α=90°   β=121.225(3)°   γ=90°

C62H44O4,CH2Cl2

C62H44O4,CH2Cl2

Cao, JingLondon, GáborDumele, Olivervon Wantoch Rekowski, MargareteTrapp, NilsRuhlmann, LaurentBoudon, CorinneStanger, AmnonDiederich, François

Journal of the American Chemical Society (2015) 137, 22 7178-7188

a=13.9753(9)Å   b=15.4590(9)Å   c=10.9343(8)Å

α=90°   β=101.803(2)°   γ=90°

C36H24N6O3

C36H24N6O3

Jayamurugan, GovindasamyFinke, Aaron D.Gisselbrecht, Jean-PaulBoudon, CorinneSchweizer, W. BerndDiederich, François

The Journal of organic chemistry (2014) 79, 1 426-431

a=7.461(2)Å   b=9.4563(13)Å   c=22.633(4)Å

α=77.902(5)°   β=87.007(7)°   γ=74.91(2)°